SRM Reports (sorted by Compound)
In the table below you will find a collection of documents concerning pesticides that are traditionally either not amenable to multiresidue methods or difficult to analyze.
Further information
» SRM Reports sorted by Report Code
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» Website with links to Method-Collections of all 4 EURLs
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List of SRM-Reports sorted by compound or compound group
| Analyte | Report Code | Short description | Link to Report |
|---|---|---|---|
| 2-Chloroethanol (2-CE) |
SRM-45 | Go to "Ethylene oxide and 2-Chloroethanol (EO and 2-CE)" | |
| 2-Phenylphenol (OPP) incl. conjugates OPP-Glucoside |
SRM-53 | Anal. Observations Report and Method: Analysis of 2-Phenylphenol (sum) via AcH-QuEChERS - involving acidic Hydrolysis - and of 2-Phenylphenol Glucoside via CEN-QuEChERS (Short Description of Anal. Observ. Report) |
Link (SRM-53) |
| 3-Hydroxy Carbofuran | SRM-23 SRM-33 SRM-44 |
Go to "Carbofuran, 3-Hydroxy" | |
| 4-Amino-3 methylbenzoic acid (Amitraz metabolite) | SRM-41 | Go to "Amitraz AO-metabolite 4-amino-3 methylbenzoic acid" | |
| 4-Hydroxy-Chlorothalonil | SRM-10 | Go to "Chlorothalonil, 4-Hydroxy" | |
| 4-Hydroxy-Mepiquat | SRM-09 | Go to "Mepiquat, 4-Hydroxy" | |
| Abamectin | SRM-01 SRM-44 |
Anal. Observations Report: Analysis of Abamectin via QuEChERS and LC-MS/MS (Short Description of Anal. Observ. Report) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-01) Link (SRM-44) |
| Acidic Pesticides (free acids) |
SRM-02 | Anal. Observations Report and Method: Analysis of Acidic Pesticides using CEN-QuEChERS and FA-QuEChERS (Short Description of Anal. Observ. Report) Compounds covered: 1-Naphthylacetic acid, 2,4,5-T, 2,4,5-TP (Fenoprop), 2,4,6-Trichlorophenol, 2,4-D, 2.4-DB, 2.4-DP (Dichlorprop), 2-Naphthoxyacetic acid, 4-CPA, Acifluorfen, Aminopyralid, Bentazon, Bromacil, Bromoxynil, BTS-9608 (Prochloraz metab.), Clopyralid, Dalapon, Dicamba, Diflufenzopyr, Dikegulac, Fenoxaprop, Fluazifop, Fluroxypyr, Gibberellic acid, Haloxyfop, Imazamox, Imazapyr, Imazethapyr, Inabenfide, Ioxynil, MCPA, MCPB, MCPP (Mecoprop), Pentachlorophenol, Picloram, Quinmerac, BH 518-2 and BH 518-4 (both Quinmerac-metab.), Quizalofop, TFNA and TFNG (both Flonicamid-metab.), Triclopyr |
Link |
| Acidic Pesticides (in Milk) |
SRM-03 | Anal. Method: Analysis of Phenoxyalkanoic Acids in Milk using QuEChERS method and LC-MS/MS A procedure for esters and conjugates is described in document SRM-43. |
Link |
| Acidic Pesticides (following Hydrolysis / Deconjugation) |
SRM-43 | Anal. Observations Report and Method: Analysis of Pesticides Entailing Conjugates or Esters in their Residue Definitions (Short Description of Anal. Observ. Report) Compounds covered: Esters: 2,4,5-T-isooctyl, 2,4-D ethylhexyl, 2,4-DB methyl, 2,4-DP ethylhexyl, Acibenzolar-S-methyl, Benazolin-ethyl, Bromoxynil-heptanoate, Carfentrazone-ethyl, Chlorthal-dimethyl, Cinidon-ethyl, Clodinafop-propargyl, Cloquintocet-mexyl, Cyhalofop-butyl, Diclofop-methyl, Fenoxaprop-ethyl, Fluazifop butyl, Fluazifop-P-butyl, Fluroxypyr meptyl, Fluroxypyr-meptyl, Haloxyfop methyl, Indole-3-acetic-acid ethyl, Ioxynil-octanoate, MCPA ethylhexyl, MCPB ethyl, MCPP trimethylpentyl, Mefenpyr-diethyl, Propaquizafop, Triclopyr-2-butoxyethyl, Trinexapac-ethyl Glucosides: 2,4-D-Glucoside, Dichlorprop-Glucoside, Haloxyfop-Glucoside, MCPA-Glucoside, OPP-glucoside Free acids measured: 2,4,5-T, 2,4-D, 2,4-DB, 2,4-DP, Bromoxynil, Cyhalofop, Dichlorprop, Diclofop, Fenoxaprop, Fluazifop, Fluroxypyr, Haloxyfop, Ioxynil, MCPA, MCPB, MCPP, Quizalofop, Triclopyr and 2-phenylphenol (OPP)
Note: The older Method SRM-04 is OBSOLETE |
Link (SRM-43) |
| Alpha-Cypermethrin | SRM-52 | Anal. Observations Report and Method: Analysis of Residues of Cypermethrin Mixtures in Food employing QuEChERS and LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Aminocyclopyrachlor | SRM-09 SRM-25 |
See QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Amitraz and DMPF | SRM-05 | Method: Analysis of Amitraz and its Main Metabolite N-2,4-Dimethylphenyl-N-Methylformamidine (DMPF) in pears via QuEChERS and LC-MS/MS | Link |
| Amitraz AO-metabolite 4-amino-3 methylbenzoic acid | SRM-41 | Anal. Observations Report and Method: Analysis of 4-Amino-3-methylbenzoic acid in eggs (the main metabolite of amitraz in products of animal origin); (Short Description of Anal. Observ. Report) | Link |
| Amitrole | SRM-09 SRM-25 SRM-44 |
See QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-09) Link (SRM-44) |
| AMTT (Metab. of tritosulfuron) | SRM-35 | Anal. Observations Report and Method: Analysis of the Tritosulfuron Metabolite AMTT by QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Azocyclotin | SRM-16 | Anal. Observations Report and Method: Analysis of Organotin-Pesticides by the QuEChERS Method - Impact of acidifying on the recoveries (Short Description of Anal. Observ. Report) Note: The previous document was withdrawn and incorporated into SRM-16 |
Link |
| BAC (Benzalokonium Chloride) | SRM-26 SRM-27 |
Go to - SRM-26: "QACs (Quarternary Ammonium Comp., DDAC C10, BAC-C8, C10, C12, C14, C16, C18)" - SRM-27: "QACs (in Milk) (DDAC C10, BAC-C10, C12, C14, C16)" |
|
| Benfuracarb | SRM-23 | Method (SRM-23): Analysis of Residues of Carbofuran (sum) using QuEChERS Method. See also: Analytical Observations Report (SRM-33): Analysis of Carbofuran (sum) by applying hydrolysis on QuEChERS extracts (Short Description of Anal. Observ. Report) |
Link (SRM-23) Link (SRM-33) |
| Bialaphos | SRM-09 SRM-25 |
See QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Bifenazate, Bifenazate-diazene |
SRM-34 | Method: Analysis of Bifenazate (sum) by QuEChERS Method using LC-MS/MS | Link |
| Boscalid metab. M510F01 | SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Bromide, Total Inorganic | SRM-06 SRM-09 SRM-25 |
Method: Bromine containing fumigants determined as Total Inorg. Bromide following derivatisation with propylene oxide, partitioning in ethyl acetate and GC analysis. For the analysis of bromide ion via LC-MS/MS please refer to the QuPPe method (PO: SRM-09; AO: SRM-25) |
Link (SRM-06) Link (SRM-44) |
| Captan / THPI | SRM-07 SRM-42 SRM-49 |
- Anal. Observ. Report + Method (SRM-07): Quantification of Residues of Captan and THPI in QuEChERS Extracts using GC-MS/MS - Anal. Observ. Report + Method (SRM-49): Analysis of the folpet degradant phthalimide and the captan degradant tetrahydrophthalimide by QuEChERS and LC-MS/MS - Anal. Observ. Report (SRM-42): Analysis of Captan, Folpet and their respective metabolites Phthalimide and Tetrahydrophthalimide via LC-MS/MS either directly or following hydrolysis Short Descriptions of Observ. Reports (SRM-07, -49, -42)
b) using standard additions |
Link (SRM-07) Link (SRM-49) Link (SRM-42) |
| Carbofuran | SRM-23 | Method (SRM-23): Analysis of Residues of Carbofuran (sum) using QuEChERS Method. See also: Analytical Observations Report (SRM-33): Analysis of Carbofuran (sum) by applying hydrolysis on QuEChERS extracts (Short Description of Anal. Observ. Report) |
Link (SRM-23) Link (SRM-33) |
| Carbofuran, 3-Hydroxy | SRM-23 SRM-33 SRM-44 |
- Method (SRM-23): Analysis of Residues of Carbofuran (sum) using QuEChERS Method. - Analytical Observations Report (SRM-33): Analysis of Carbofuran (sum) by applying hydrolysis on QuEChERS extracts (Short Description of Anal. Observ. Report) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-23) Link (SRM-33) |
| Carbosulfan | SRM-23 SRM-33 |
Method (SRM-23): Analysis of Residues of Carbofuran (sum) using QuEChERS Method. See also: Analytical Observations Report (SRM-33): Analysis of Carbofuran (sum) by applying hydrolysis on QuEChERS extracts See Short Description of Anal. Observ. Report |
Link (SRM-23) Link (SRM-33) |
| Chlorate | SRM-09 SRM-25 SRM-44 |
See QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2) |
Link (SRM-09) Link (SRM-44) |
| Chloridazon-desphenyl | SRM-51 SRM-09 SRM-25 |
Anal. Observations Report: Analysis of chloridazon-desphenyl in case of interfering matrix in LC-MS/MS to avoid false positives, e.g. in honey (Short Description of Anal. Observ. Report) See also QuPPe method (PO: SRM-09; AO: SRM-25) |
Link (SRM-51) Link (SRM-09) |
| Chlormequat | SRM-08 SRM-09 SRM-25 |
Method: Analysis of Chlormequat and Mepiquat Residues in Foods of Plant Origin; See also: QuPPe method (PO: SRM-09; AO: SRM-25) |
Link Link |
| Chlorothalonil | SRM-10 | Method: Modified QuEChERS-Method for the Analysis of Chlorothalonil in Fruits and Vegetables | Link |
| Chlorothalonil, 4-Hydroxy (SDS-3701) | SRM-28 SRM-10 |
Method: Analysis of 4-Hydroxy-Chlorothalonil (SDS-3701) in Milk. For the analysis of SDS-3701 in fruits and vegetables check SRM-10 |
Link |
| Cyhalothrin, Lambda- / Gamma- |
SRM-39 SRM-44 |
- Method (SRM-39): Analysis of Lambda- and Gamma-Cyhalothrin involving QuEChERS Extraction and Enantioselective LC-Separation of RS and SR-Isomers (QuEChERS-based procedure involving enantioselective LC-MS/MS analysis of the two isomers of lambda-cyhalothrin. Separation on a cellulose-based stationary phase) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-39) |
| Cyhexatin | SRM-16 | Anal. Observations Report and Method: Analysis of Organotin-Pesticides by the QuEChERS Method - Impact of acidifying on the recoveries (Short Description of Anal. Observ. Report) Note: The previous document was withdrawn and incorporated into SRM-16 |
Link |
| Cypermethrin | SRM-52 | Go to Alpha Cypermethrin | |
| Cyromazine | SRM-09 | See QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Daminozide | SRM-09 | See QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| DDAC (Didecyldimethyl-ammonium chloride) | SRM-26 SRM-27 |
Go to - SRM-26: "QACs (Quarternary Ammonium Comp., DDAC C10, BAC-C8, C10, C12, C14, C16, C18)" - SRM-27: "QACs (in Milk) (DDAC C10, BAC-C10, C12, C14, C16)" |
|
| Diclofop | SRM-44 | Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-44) |
| Dicofol | SRM-11 | See Short Description of Anal. Observ. Report | Link |
| Diethanolamine | SRM-09 | See QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Difenzoquat and N,N-Dimethylhydrazine | SRM-09 | See QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Difluoroacetic acid (DFA) | SRM-09 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) - Residue Findings Report: Residues of DFA and TFA in Samples of Plant Origin (Link) |
Link (SRM-09) Link (SRM-44) |
| Dimethoate and Omethoate metabolites (III, X, XI, XII, XX and XXIII) | SRM-40 SRM-09 |
Anal. Observations Report and Method: Analysis of Dimethoate and Omethoate Metabolites - Method Development and Pilot Monitoring (Short Description of Anal. Observ. Report) |
Link (SRM-40) Link (SRM-09) |
| Dimoxystrobin metab. 505M09 | SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Diquat | SRM-09 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-09) Link (SRM-44) |
| Dithianon | SRM-12 | Method: Analysis of Dithianon in Fruits and Vegetables using acidified QuEChERS and LC-MS/MS. Analytical observations report SRM-13 gives background information on this method (Short Description of Anal. Observ. Report) |
Link (SRM-12) Link (SRM-13) |
| Dithiocarbamates as CS2 | SRM-14 | Analytical Observations Report and Method: Analysis of residues of dithiocarbamate fungicides in low-oil content food of plant origin involving cleavage into carbon disulfide, partitioning into isooctane and measurement by GC-MS/MS or GC-ECD. (Short Description of Anal. Observ. Report) |
Link |
| Dodine | SRM-15 | Analytical Observations Report: Analysis of Dodine by the QuEChERS Method - Interactions in the injector and role of matrix. See Short Description of Anal. Observ. Report |
Link |
| Emamectin | SRM-44 | Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-44) |
| Ethephon | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Ethoxyquin | SRM-21 (PO), SRM-24 (AO) |
- Analytical Observations Report and Method: Improvement of Ethoxyquin Recoveries by QuEChERS Through the Addition of Ascorbic Acid (SRM-21 for food of plant origin) - Analytical Observations Report and Method: Analysis of Ethoxyquin and its Metabolites in Fish using the QuEChERS Method (SRM-24 for food of plant origin) Short Descriptions of Anal. Observ. Reports (SRM-21, -24) |
Link (SRM-21) Link (SRM-24)
|
| Ethoxyquin Dimer | SRM-44 | Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-44) |
| Ethylene oxide and 2-Chloroethanol (EO and 2-CE) |
SRM-45 | Anal. Observations Report and Method: Analysis of Ethylene Oxide and its Metabolite 2-Chloroethanol by the QuOil or the QuEChERS Method and GC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| ETU | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Fenbutatin oxide | SRM-16 | Anal. Observations Report and Method: Analysis of Organotin-Pesticides by the QuEChERS Method - Impact of acidifying on the recoveries (Short Description of Anal. Observ. Report) Note: The previous document was withdrawn and incorporated into SRM-16 |
Link |
| Fenpropidin metab. CGA289267 | SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Fenpropimorph carboxylic acid (BF-421-2) | SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Fentin | SRM-16 SRM-44 |
Anal. Observations Report and Method: Analysis of Organotin-Pesticides by the QuEChERS Method - Impact of acidifying on the recoveries (Short Description of Anal. Observ. Report) Note: The previous document was withdrawn and incorporated into SRM-16 See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link |
| Flonicamid Metabolites (TFNA, TFNG, TFNA-AM) | SRM-17 SRM-02 |
Validation Report: Validation of Flonicamid-Metabolites (TFNA, TFNG, TFNA-AM) using QuEChERS method See also: SRM-02 for the comparison between CEN-QuECHERS and FA-QuEChERS |
Link (SRM-17) |
| Fluoride ion | SRM-50 | Anal. Observations Report and Method: Determination of fluoride ion with direct measurement and/or following microdiffusion using ion selective electrodes (ISE) See short Description of Anal. Observ. Report |
Link |
| Fosetyl Aluminium (detected as Fosetyl) | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Folpet / PI (Phthalimide) | SRM-07 SRM-42 SRM-49 |
- Anal. Observ. Report + Method (SRM-07): Quantification of Residues of Captan and THPI in QuEChERS Extracts using GC-MS/MS - Anal. Observ. Report + Method (SRM-49): Analysis of the folpet degradant phthalimide and the captan degradant tetrahydrophthalimide by QuEChERS and LC-MS/MS - Anal. Observ. Report (SRM-42): Analysis of Captan, Folpet and their respective metabolites Phthalimide and Tetrahydrophthalimide via LC-MS/MS either directly or following hydrolysis Short Descriptions of Anal. Observ. Reports (SRM-07, -42, -49) See also: b) using standard additions |
Link (SRM-07) Link (SRM-49) Link (SRM-42) |
| Fumigants | SRM-29 | Method (SRM-29): Analysis of Fumigants in Cereals and Dry Fruits Applying GC-MS/MS Publication (Link): Analysis of Fumigants in Cereals and Dried Fruits: Part 1 via GC-MS/MS Compounds covered: Trichloroethylene, ethylene chlorobromide, 1,3-dichloropropene (cis+trans), tetrachloroethylene, 1,1,2,2-tetrachloroethane, p-dichlorobenzene, naphthalene, 1,2-dibromo-3-chloropropane, dichlorvos, p-nitrochlorobenzene, azobenzene, chloropicrin, ethylene dibromide |
Link (SRM-29) Link (publication) |
| Furathiocarb | SRM-23 SRM-33 |
Method (SRM-23): Analysis of Residues of Carbofuran (sum) using QuEChERS Method. See also: Analytical Observations Report (SRM-33): Analysis of Carbofuran (sum) by applying hydrolysis on QuEChERS extracts See Short Description of Anal. Observ. Report |
Link (SRM-23) Link (SRM-33) |
| Glufosinate | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| N-Acetyl glufosinate | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| MPPA (glufosinate metabolite) |
SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Glyphosate | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| N-Acetyl-glyphosate (glyphosate metabolite) | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| AMPA (glyphosate metabolite) |
SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| N-Acetyl-AMPA (glyphosate metabolite) | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Guazatine | SRM-38 | Anal. Observations Report: Analysis of Guazatine in Food Products (Short Description of Anal. Observ. Report) | Link |
| Haloxyfop | SRM-02 SRM-03 SRM-43 SRM-44 |
- Analytical Observ. Report and Method (SRM-02): Analysis of Acidic Pesticides using CEN-QuEChERS and FA-QuEChERS (Short Description of Anal. Observ. Report) - Analytical Method (SRM-03): Analysis of Phenoxyalkanoic Acids in Milk using QuEChERS method and LC-MS/MS - Analytical Observ. Report and Method (SRM-43): Analysis of Pesticides Entailing Conjugates or Esters in their Residue Definitions (Short Description of Anal. Observ. Report) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-02) Link (SRM-03) Link (SRM-43) Link (SRM-44) |
| HEPA (ethephon metabolite) |
SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Isoxaflutole metab. RPA202248 and RPA203328 |
SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Kasugamycin | SRM-09 | QuPPe method (PO: SRM-09; AO: SRM-25) | |
| Maleic hydrazide | SRM-09 | QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Mepiquat | SRM-08 SRM-09 SRM-25 |
Method: Analysis of Chlormequat and Mepiquat Residues in Foods of Plant Origin; See also: QuPPe method (PO: SRM-09; AO: SRM-25) |
Link (SRM-08)
|
| Mepiquat, 4-Hydroxy | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Meptyldinocap | SRM-47 | Anal. Observations Report and Method: Analysis of Meptyldinocap by QuEChERS followed by alkaline hydrolysis and LC-MS/MS measurement (Short Description of Anal. Observ. Report) | Link |
| Morpholine | SRM-09 | QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Nereistoxin | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Nicotine | SRM-09 SRM-25 SRM-30 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Anal. Observations Report and Method (SRM-30): Analysis of Nicotine in Mushrooms using QuEChERS under alkaline conditions - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-30) Link (SRM-09) Link (SRM-44) |
| Omethoate metabolites | SRM-40 | Go to "Dimethoate and Omethoate metabolites (III, X, XI, XII, XX and XXIII)" | |
| Organophosphorous Pesticides; Polar Metabolites of ~ O,O-dimethyl thiophosphate O,O-dimethyl dithiophosphate Dimethyl phosphate |
SRM-09 | QuPPe method (PO: SRM-09; AO: SRM-25) Note: For metabolites of Dimethoate / Omethoate go to "Dimethoate and Omethoate metabolites (III, X, XI, XII, XX and XXIII)" |
Link (SRM-09) |
| Organotins | SRM-16 | Anal. Observations Report and Method: Analysis of Organotin-Pesticides by the QuEChERS Method - Impact of acidifying on the recoveries (Short Description of Anal. Observ. Report) Note: The previous document was withdrawn and incorporated into SRM-16 |
Link |
| Paraquat | SRM-09 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-09) Link (SRM-44) |
| PCP | SRM-31 | Method: Analysis of Pentachlorophenol (PCP) in guar gum by modified QuEChERS method; Take note: Commission Decision of 29 April 2008 imposing special conditions governing guar gum originating in or consigned from India due to contamination risks of those products by pentachlorophenol and dioxins: 2008/352/EC |
Link |
| Perchlorate | SRM-09 SRM-25 SRM-44 |
See QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-09) Link (SRM-44) |
| Phosphine | SRM-18 | Method: Analysis of the Fumigant Phosphine by applying Headspace-GC-MSD | Link (SRM-18) Link (e-journal) |
| Phosphonic acid (plant strengthener and Fosetyl degradant) | SRM-09 SRM-25 SRM-44 |
See QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-09) Link (SRM-44) |
| Prochloraz | SRM-19 | Anal. Observations Report and Method: Determination of Prochloraz (sum) via its Metabolites (Short Description of Anal. Observ. Report) | Link |
| Prochloraz Metabolites BTS 44596, BTS 44596, BTS 40348, BTS 9608, 2,4,6-Trichlorophenol |
SRM-19 | Anal. Observations Report and Method: Determination of Prochloraz (sum) via its Metabolites (Short Description of Anal. Observ. Report) | |
| Propamocarb | SRM-09 SRM-25 SRM-20 |
Anal. Observation Report: Matrix-induced Signal Enhancement of Propamocarb in LC-MS/MS (Short Description of Anal. Observ. Report) See also: QuPPe method (PO: SRM-09; AO: SRM-25) |
Link (SRM-20) Link (SRM-09) |
| Propineb (via Propylene diamine) | SRM-48 SRM-09 |
Anal. Observation Report: Intermediate analytical observations as regards the analysis of propineb as propylenediamine following reductive cleavage with HCl/SnCl2 and measurement via ion-pair LC-MS/MS (Short Description of Anal. Observ. Report) See also: QuPPe method (PO: SRM-09; AO: SRM-25) |
Link |
| PTU | SRM-09 SRM-25 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-09) Link (SRM-44) |
| Pyridate | SRM-22 | Anal. Observation Report and Method: Analysis of Pyridate and its metabolite Pyridafol by QuEChERS and LC-MS/MS (Short Description of Anal. Observ. Report) Note: This method was not designed for pyridafol conjugates |
Link |
| Pymetrozine | SRM-32 | Anal. Observation Report and Method: Analysis of Pymetrozine by the QuEChERS Method - Impact of pH on Recovery Rate (Short Description of Anal. Observ. Report) | Link |
| QACs (Quarternary Ammonium Comp.) (DDAC C10, BAC-C8, C10, C12, C14, C16, C18) |
SRM-26 | Anal. Observation Report and Method: Analysis of Didecyldimethylammonium chloride (DDAC-C10) and Benzalkonium chloride (BAC-C10; BAC-C12; BAC-C14; BAC-C-16) by applying the QuEChERS method without cleanup and LC-MS/MS determination (ESI-positive mode). (Short Description of Anal. Observ. Report) |
Link |
| QACs (in Milk) (DDAC C10, BAC-C10, C12, C14, C16) |
SRM-27 | Method: Analysis of DDAC-C10 and BAC (BAC-C10; BAC-C12; BAC-C14; BAC-C-16) in milk by applying the QuEChERS method without cleanup and LC-MS/MS determination (ESI-positive mode). | Link |
| Spiroxamine carboxylic acid | SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Streptomycin | SRM-09 | QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Sulfuryl fluoride | SRM-37 | Anal. Observation Report and Method: Analysis of the Fumigant Sulfuryl Fluoride Applying Headspace-GC-MSD (Short Description of Anal. Observ. Report) |
Link |
| TFNA and TFNG (Metabolites of Flonicamid) | SRM-14 | Go to "Flonicamid Metabolites (TFNA, TFNG, TFNA-AM)" | |
| Topramezone | SRM-44 | Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) |
Link (SRM-44) |
| Triazole Derivative Metabolites (TDMs) Triazole-acetic acid Triazole-alanine Triazole-lactic acid 1,2,4-Triazole |
SRM-09 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) - Publication: "Determination of Triazole Derivative Metabolites (TDMs) in Fruit and Vegetables using the QuPPe Method and Differential Mobility Spectrometry (DMS) and Survey of the Residue Situation in Organic and Conventional Produce" (Link) |
Link (SRM-09) Link (SRM-44) Link (publication) |
| Triethanolamine | SRM-09 | QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
| Trifloxystrobin metab. CGA 321113 | SRM-36 | Anal. Observations Report and Method: Analysis of various relevant pesticide metabolites of in products of animal origin by the QuEChERS Method using LC-MS/MS (Short Description of Anal. Observ. Report) | Link |
| Trifluoroacetic acid | SRM-09 SRM-25 SRM-44 |
QuPPe method (PO: SRM-09; AO: SRM-25) See also: - Analysis in infant formulae + milk: a) Method (SRM-44); Short Description of SRM-44 b) Pilot Monitoring Report (Part 2)) - Residue Findings Report: Residues of DFA and TFA in Samples of Plant Origin (Link) |
Link (SRM-09) Link (SRM-44) |
| Trimesium (trimethylsulfonium cation) | SRM-09 SRM-25 |
QuPPe method (PO: SRM-09; AO: SRM-25) | Link (SRM-09) |
Additional documents on analytical topics
Strategy of EURL-SRM method development activities
Impact of various factors on the extractability of incurred pesticide residues
Collection of Analytical Observations
Excel file for the calculation Captan/THPI and Folpet/Phthalimide using external calibration
(see Description of Procedure)
Excel file for the calculation Captan/THPI and Folpet/Phthalimide using standard additions
Last update: 06.04.2017
(see Description of Procedure)
Workflow to perform quantification by standard addition procedure
Standard addition is an effective way to compensate for matrix effects, e.g. in cases of "difficult" matrix-pesticide combinations or if no blank matrix is available for external matrix matched calibration. Standard addition can be performed either to aliquots of the sample extract or direct to analytical portions prior to extraction. In the first case, it only corrects for matrix effects as well as for analyte degradation in the extract, the latter case, it also corrects for recovery during extraction and clean-up. Because of linear extrapolation linearity of response throughout the measured concentration range is paramount. Furthermore it should be considered, that added amounts are not too small in order to reduce the influence of measurement variability on the slope of the linear regression.
Excel file Standard Addition to Extract Aliquots
Excel file Standard Addition to Sample Portions
Last modified 27-02-2025, 21:56:22
Published 25-04-2016, 08:18:21
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